Development of a method for total Hg determination in oil samples by cold vapor atomic absorption spectrometry after its extraction induced by emulsion breaking
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چکیده
منابع مشابه
Cold Vapor Atomic Absorption Determination of Hg in Crude Oil and Gasoline Samples after Solid Phase Extraction Using Modified Disks
A facile and highly efficient method have been developed for the preconcentration of the mercury content in crude oil and gasoline samples after digestion with microwave-assisted digestion. Octadecyl silica membrane disk has been modified by the recently synthesized triazene ligand, (E)-1-(2-ethoxyphenyl)-3-(4-nitrophenyl) triaz-1-ene (ENT), then the modified membrane was used for the preco...
متن کاملcold vapor atomic absorption determination of hg in crude oil and gasoline samples after solid phase extraction using modified disks
a facile and highly efficient method have been developed for the preconcentration of the mercury content in crude oil and gasoline samples after digestion with microwave-assisted digestion. octadecyl silica membrane disk has been modified by the recently synthesized triazene ligand, (e)-1-(2-ethoxyphenyl)-3-(4-nitrophenyl) triaz-1-ene (ent), then the modified membrane was used for the preconcen...
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A new method for the determination of trace copper(II) in food samples by Cloud Point Extraction(CPE) combined with Flame Atomic Absorption Spectrometry(FAAS) is presented and evaluated. The method is based on the fact that hydrophobic complex of copper(II) with sodium diethyldithiocarbamate (DDTC) was formed at pH 6.0 and subsequently the hydrophobic complex was extracted into surfactant-r...
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Um método simples e robusto para a determinação de Hg em amostras ambientais por espectrometria de absorção atômica com geração de vapor frio diretamente de suspensões ácidas é proposto. Após redução do tamanho das partículas da amostra para ≤ 50 μm em gral de ágata, dois procedimentos foram utilizados para a preparação das suspensões: com 6,7% v/v de ácido nítrico ou 10% v/v de água-régia mais...
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ژورنال
عنوان ژورنال: Talanta
سال: 2015
ISSN: 0039-9140
DOI: 10.1016/j.talanta.2014.10.019